ASTM D335909 标准试验方法 胶带法测量附着力.doc

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1、Designation: D 3359 02名称： D 3359-02Standard Test Methods forMeasuring Adhesion by Tape Test1ASTM D3359-09 标准试验方法 胶带法测量附着力This standard is issued under the fixed designation D 3359; the number immediately following the designation indicates the year of original adoption or, in the case of revision, t

2、he year of last revision. A number in parentheses indicates the year of last reapproval. A superscript epsilon (e) indicates an editorial change since the last revision or reapproval.这个标准是D 3359确定了以后发行的。数字代表名称最初通过的时间，或者修订情况，和最新版本。括号内的数字代表最新重新审批时间。上标代表最新版本的变化或重新审批。This standard has been approved for

3、use by agencies of the Department of Defense.该标准已经被国防机构部门批准使用。1. Scope 范围1.1 These test methods cover procedures for assessing the adhesion of coating films to metallic substrates by applying and removing pressure-sensitive tape over cuts made in the film.本标准提出的试验方法是规定通过在漆膜切割区施加和撕离压敏胶带的方式，对漆膜与金属底材之间

4、的附 着力进行评定的程序1.2 Test Method A is primarily intended for use at job sites while Test Method B is more suitable for use in the laboratory. Also, Test Method B is not considered suitable for films thicker than 5 mils (125m).试验方法A主要是供工作场所用，而试验方法B更适合实验室使用。试验方法B被视为不适合厚度超过 5毫英寸（125微米）的漆膜。NOTE 1Subject to a

5、greement between the purchaser and the seller,Test Method B can be used for thicker films if wider spaced cuts are employed.注 1-根据买卖双方的协议，如果切割间距较宽，漆膜较厚时可采用试验方法B。1.3 These test methods are used to establish whether the adhesion of a coating to a substrate is at a generally adequate level. They do not

6、 distinguish between higher levels of adhesion for which more sophisticated methods of measurement are required.本标准规定的试验方法用于总体判定涂层与底材之间的附着力是否达到足够的水平。如果附着力较高，本标准规定的试验方法无法精确地区分附着力的差别，需要使用更精确的测量方法。NOTE 2It should be recognized that differences in adherability of the coating surface can affect the resul

7、ts obtained with coatings having the same inherent adhesion.注2-应该注意到，涂层内在附着力相同的情况下，涂覆面附着性的差别会影响测量结果。1.4 In multicoat systems adhesion failure may occur between coats so that the adhesion of the coating system to the substrate is not determined.多层涂层体系可能出现层间脱落，无法确定涂层体系与底材之间的附着力。1.5 The values stated i

8、n SI units are to be regarded as the standard. The values given in parentheses are for information only.SI单位的数值被视为标准，括号内的数值仅供参考.1.6 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appro

9、priate safety and health practices and determine the applicability of regulatory limitations prior to use.本标准并没有指出与其使用相关的所有安全事项。本标准的用户应负责在使用之前采取适当的安全和卫生 措施，并确定各项管理限制条件的适用性2. Referenced Documents 参考文件2.1 ASTM Standards: 美国材料与试验协会标准D 609 Practice for Preparation of Cold-Rolled Steel Panels for Testing

10、 Paint, Varnish, Conversion Coatings, and Related Coating Products2D609-涂料,清漆,转化涂层和相关覆层产品的测试-用冷轧钢板制备的标准实施规范D 823 Practices for Producing Films of Uniform Thickness of Paint, Varnish, and Related Products on Test Panels2D823-色漆,清漆,喷漆及有关产品制成厚度均匀漆膜试片的方法D 1000 Test Method For Pressure-Sensitive Adhesive

11、-Coated Tapes Used for Electrical and Electronic Applications3D1000-电气设备用压合敏感胶粘剂涂覆带的试验方法D 1730 Practices for Preparation of Aluminum and Aluminum-Alloy Surfaces for Painting4D1730- 涂漆用铝和铝合金表面预处理标准实施规范D 2092 Guide for Preparation of Zinc-Coated (Galvanized) Steel Surfaces for Painting5D2092-用于涂漆的镀锌钢材

12、表面预处理的标准指南D 2370 Test Method for Tensile Properties of Organic Coatings2D2370-有机涂层抗拉性能的标准试验方法。D 3330 Test Method for Peel Adhesion of Pressure-Sensitive Tape 6D3330- 压敏胶带剥离强度测试标准D 3924 Specification for Standard Environment for Conditioning and Testing Paint, Varnish, Lacquer, and Related Materials2

13、D 3924-色漆,清漆,喷漆和相关物质状态调节和试验用标准环境规范D 4060 Test Method for Abrasion Resistance of Organic Coatings by the Taber Abraser2D 4060 -用泰伯尔磨蚀机测定有机涂层耐磨性的标准试验方法 3. Summary of Test Methods 试验方法摘要3.1 Test Method AAn X-cut is made through the film to the substrate, pressure-sensitive tape is applied over the cut

14、and then removed, and adhesion is assessed qualitatively on the 0 to 5 scale.试验方法A：一个X切口贯通漆膜和底材 ，在切口处施加和移除压敏胶带，粘附力按照0-5等级进行评估。3.2 Test Method BA lattice pattern with either six or eleven cuts in each direction is made in the film to the substrate, pressure-sensitive tape is applied over the lattice

15、andthen removed, and adhesion is evaluated by comparison with descriptions and illustrations.试验方法B：在涂层与底材之间切割出六道或十一道格形状的切痕，在格之间施加和移除压敏胶带，通过图表描述对比来评估粘附力。4. Significance and Use 意义和用途4.1 If a coating is to fulfill its function of protecting or decorating a substrate, it must adhere to it for the expec

16、ted service life. Because the substrate and its surface preparation (or lack of it) have a drastic effect on the adhesion of coatings, a method to evaluate adhesion of a coating to different substrates or surface treatments, or of different coatings to the same substrate and treatment, is of conside

17、rable usefulness in the industry.如果涂层能保护或装饰底材，必须要达到预期的服务寿命。因为涂层的附着性对底材和其表面处理（或缺乏）有强烈的影响，用同一种方法来评估不同底材涂层或表面处理，或同一底材和表面处理但不同涂层被视为无用1 These test methods are under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and are the direct responsibility of Subco

18、mmittee D01.23 on Physical Properties of Applied Paint Films.Current edition approved Aug. 10, 2002. Published October 2002. Originally published as D 3359 74. Last previous edition D 3359 97.2 Annual Book of ASTM Standards, Vol 06.01.3 Annual Book of ASTM Standards, Vol 10.01.4 Annual Book of ASTM

19、Standards, Vol 02.05.5 Annual Book of ASTM Standards, Vol 06.02.6 Annual Book of ASTM Standards, Vol 15.09.此测试方法在美国材料与试验协会D01是关于油漆和相关涂层、材料、应用软件和关于油漆涂层的物理性能D01.23的权限下进行的。最新版本在2002年8月10号被认可。2002年10月出版。最初出版是D3359-74，上一个版本是D3359-97。4.2 The limitations of all adhesion methods and the specific limitation

20、of this test method to lower levels of adhesion (see1.3) should be recognized before using it. The intra- and inter-laboratory precision of this test method is similar to other widely-accepted tests for coated substrates (for example, Test Method D 2370 and Test Method D 4060), but this is partly th

21、e result of it being insensitive to all but large differences in adhesion. The limited scale of 0 to 5 was selected deliberately to avoid a false impression of being sensitive.在使用前，应承认所有附着力方法的局限性和这个试验方法对较低级附着力（见1.3）的特殊限制。内部多个实验室所进行的精密度的这种测试方法类似于其他已被广泛接受涂层测试(如测试方法D2370及测试方法D4060),为避免敏感的假象而刻意限定0-5等级范围

22、。TEST METHOD AX-CUT TAPE TEST 试验方法A：划X法胶带测试5. Apparatus and Materials 仪器和材料5.1 Cutting ToolSharp razor blade, scalpel, knife or other cutting devices. It is of particular importance that the cutting edges be in good condition.切削刀具：锋利的刀片、手术刀、刀或者其他切削设备。5.2 Cutting GuideSteel or other hard metal straig

23、htedge to ensure straight cuts.引导切割钢制或其他金属制的直尺或夹具来保证直线切割。5.3 Tape25-mm (1.0-in.) wide semitransparent pressure sensitive tape7 with an adhesion strength agreed upon by the supplier and the user is needed. Because of the variability in adhesion strength from batch-to-batch and with time, it is essent

24、ial that tape from the same batch be used when tests are to be run in different laboratories. If this is not possible， the test method should be used only for ranking a series of test coatings.胶带经供应商和用户同意的25mm宽的半透明的透明具有粘合力压敏胶粘带。因为粘合力是随着时间和批次不同是变化的，故各个实验室进行测试时所使用的胶带要是同一批次的。如果无法做到这一点，此测试方法应仅适用于一系列涂层测试

25、的排名。5.4 Rubber Eraser, on the end of a pencil.铅笔一头的橡皮擦5.5 IlluminationA light source is helpful in determining whether the cuts have been made through the film to the substrate.照明灯源（如手电筒）当在漆膜与底材之间开有切割时，光源是有很有帮助的。6. Test Specimens 试样6.1 When this test method is used in the field, the specimen is the

26、coated structure or article on which the adhesion is to be evaluated.当这个试验方法在实地使用时，被测试的结构或物品上的粘附力都将要被评估。6.2 For laboratory use apply the materials to be tested to panels of the composition and surface conditions on which it is desired to determine the adhesion.实验室使用申请材料进行试验,通过测试板的成份的和表面情况来评估附着力。NOTE

27、 3Applicable test panel description and surface preparation methods are given in Practice D 609 and Practices D 1730 and D 2092.备注3：适用的测试板描述和表面处理方法见D 609和D 1730、D 2092。NOTE 4Coatings should be applied in accordance with Practice D 823, or as agreed upon between the purchaser and the seller.备注4：涂层应按照

28、D 823，或者买方和卖方之间所达成的协议。NOTE 5If desired or specified, the coated test panels may be subjected to a preliminary exposure such as water immersion, salt spray, or high humidity before conducting the tape test. The conditions and time of exposure will be governed by ultimate coating use or shall be agree

29、d upon between the purchaser and seller.备注5：如需要或已列明，规定，涂层测试板在进行测试前可能需先暴露于/ 如：浸在水中，盐雾或高湿度中。浸泡的时间和条件应取决于涂层产品的最终用途或者买方和卖方之间达成的协议。7. Procedure 程序7.1 Select an area free of blemishes and minor surface imperfections. For tests in the field, ensure that the surface is clean and dry. Extremes in temperature

30、 or relative humidity may affect the adhesion of the tape or the coating.在实地做此试验时，需确保试样涂层表面要清洁干燥。高温和高湿会影响胶带附着力。7.1.1 For specimens which have been immersed: After immersion, clean and wipe the surface with an appropriate solvent which will not harm the integrity of the coating. Then dry or prepare t

31、he surface, or both, as agreed upon between the purchaser and the seller.根据买方和卖方之间双方达成的协议，对于被浸泡的样件，浸泡完以后用适当的溶剂（不能损害涂层）擦净表面，然后让其干燥7.2 Make two cuts in the film each about 40 mm (1.5 in.) long that intersect near their middle with a smaller angle of between 30 and 45. When making the incisions, use th

32、estraightedge and cut through the coating to the substrate in one steady motion.用刀具沿直线稳定地切割漆腊至底材，夹角30-45，划线40mm长，交叉点在线长的中间7.3 Inspect the incisions for reflection of light from the metal substrate to establish that the coating film has been penetrated. If the substrate has not been reached make anot

33、her X in a different location. Do not attempt to deepen a previous cut as this may affect adhesion along the incision.用灯光照明查看钢质基底的反射，确定划痕是否到底材，如果没有，在不同位置再划一个X。不要试图加深以前切口的深度，这样可能影响切口处的附着性。7.4 Remove two complete laps of the pressure-sensitive tape from the roll and discard. Remove an additional lengt

34、h at a steady (that is, not jerked) rate and cut a piece about 75 mm (3 in.) long.除去压敏胶带上面的两圈，然后以稳定的速率拉开胶带，剪下长约75mm胶带。7.5 Place the center of the tape at the intersection of the cuts with the tape running in the same direction as the smaller angles. Smooth the tape into place by finger in the area o

35、f the incisions and then rub firmly with the eraser on the end of a pencil. The color under the transparent tape is a useful indication of when good contact has been made.把胶带中间放在切割处的交叉点上，用手指压平，为了保证胶带与涂层接触良好，再用铅笔顶端的橡皮擦用力摩平胶带，透过透明胶带析颜色可以帮助我们看出与漆膜接触的状态密实程度7.6 Within 90 30 s of application, remove the t

36、ape by seizing the free end and pulling it off rapidly (not jerked) back upon itself at as close to an angle of 180 as possible.在贴上胶带9030 秒内，扯住胶带悬空的一端，快速地并尽可能确保拉力沿180的方向进行撕离胶带。7.7 Inspect the X-cut area for removal of coating from the substrate or previous coating and rate the adhesion in accordance

37、 with the following scale:按照下列标准进行检查底材涂层脱落的X切口面积情况:5A No peeling or removal,没有脱皮或脱皮4A Trace peeling or removal along incisions or at their intersection,沿刀痕或在其交叉口处有脱皮或脱落的痕迹3A Jagged removal along incisions up to 1.6 mm (1/16 in.) on either side,刀痕两边都有缺口状脱落达1.6mm2A Jagged removal along most of incisio

38、ns up to 3.2 mm (1/8 in.) on either side,刀痕两边都有缺口状脱落达3.2mm1A Removal from most of the area of the X under the tape, 胶带下的X区域内大部分脱落0A Removal beyond the area of the X.脱落面各超出X区域。7.8 Repeat the test in two other locations on each test panel. For large structures make sufficient tests to ensure that the

39、adhesion evaluation is representative of the whole surface.在每个测试板的另外两个地方重复测试。对大型结构需充分试验以保证了粘合力评估以代表整个表面。7.9 After making several cuts examine the cutting edge and, if necessary, remove any flat spots or wire-edge by abrading lightly on a fine oil stone before using again. Discard cutting tools that

40、develop nicks or other defects that tear the film.切割了几个切口以后，检查切口边，如果需要，使用以前用油石轻微磨擦去除斑点、除尖角Report 报告8.1 Report the number of tests, their mean and range, and for coating systems, where the failure occurred that is, between first coat and substrate, between first and second coat, etc.记录试验的数次及相关意思和范围，对

41、于涂层系统，失效发生在哪里，发生在第一个涂层和基体之间，还是在第一与第二涂层之间。8.2 For field tests report the structure or article tested, the location and the environmental conditions at the time of testing.实地测试时，报告需注明涂层系统、施工时间、固化情况。8.3 For test panels report the substrate employed, the type of coating, the method of cure, and the envi

42、ronmental conditions at the time of testing.记录测试板所用的底材，涂层的类型，处理的方法，和试验时的环境情况。8.4 If the adhesion strength of the tape has been determined in accordance with Test Methods D 1000 or D 3330, report the results with the adhesion rating(s). If the adhesion strength of the tape has not been determined, re

43、port the specific tape used and its manufacturer.如果胶带的附着力已确定符合D 1000 或者 D 3330，记录附着力等级的结果。如果胶带附着力大小未确定，记录所使用的胶带细节及其生产厂家。8.5 If the test is performed after immersion, report immersion conditions and method of sample preparation.如果试验在浸泡以后再进行，记录浸泡的条件和试样准备方法。9. Precision and Bias 8 精度和偏差9.1 In an interl

44、aboratory study of this test method in which operators in six laboratories made one adhesion measurement on three panels each of three coatings covering a wide range of adhesion, the within-laboratories standard deviation was found to be 0.33 and the between-laboratories 0.44. Based on these standar

45、d deviations, the following criteria should be used for judging the acceptability of results at the 95 % confidence level:在多个实验室进行的测试方法。操作者在6个实验室内的3个平板上（各涂层上进行一系列附着力测量，做同一个附着力测试。在同一个实验室的标准偏差为0.33,在不同实验室发现偏差为0.44.以这些标准偏差为基础，以下标准应该用来确定结果的可行性有95%的可信度。9.1.1 RepeatabilityProvided adhesion is uniform over

46、 a large surface, results obtained by the same operator should be considered suspect if they differ by more than 1 rating unit for two measurements.重复性：假定在一个大表面的附着力是一致的，同一个操作者两次测量得到的结果差异超过一个单位等级，那麽将被认为是不可信的。9.1.2 ReproducibilityTwo results, each the mean of triplicates, obtained by different operato

47、rs should be considered suspect if they differ by more than 1.5 rating units.再现性：取每个操作者3次测量的均值，如果得到的两个结果超过1.5个单位等级，那麽将被认为是不可信的。9.2 Bias cannot be established for these test methods.用这些测试方法不能确定偏差。TEST METHOD BCROSS-CUT TAPE TEST 测试方法B：划格法胶带测试10. Apparatus and Materials 器具和材料10.1 Cutting Tool9Sharp ra

48、zor blade, scalpel, knife or other cutting device having a cutting edge angle between 15 and 30 that will make either a single cut or several cuts at once. It is of particular importance that the cutting edge or edges be in good condition.切割刀具：锋利的刀刃、手术刀、刀或者其他切削设备（刀刃在15-30度之间），切削单个切口或多个切口。切割边缘情况良好是特别重要的。10.2 Cutting GuideIf cuts are made manually (as opposed to a mechanical apparatus) a steel or other hard metal straightedge or template to ensure straight cuts.切割指南：如果是手动切削，钢制或其他金属制的直尺